3C27
Cyanofluorophenylacetamides as Orally Efficacious Thrombin Inhibitors
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | MACSCIENCE |
Detector technology | CCD |
Collection date | 2002-06-07 |
Detector | BRUKER SMART 6000 |
Wavelength(s) | 1.54 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 70.854, 72.026, 72.987 |
Unit cell angles | 90.00, 100.50, 90.00 |
Refinement procedure
Resolution | 50.075 - 2.182 |
R-factor | 0.176 |
Rwork | 0.174 |
R-free | 0.21500 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.232 |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.075 |
High resolution limit [Å] | 2.182 |
Number of reflections | 18406 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |