3BWE
Crystal structure of aggregated form of DJ1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-11-04 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.12714 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 193.616, 102.582, 85.535 |
Unit cell angles | 90.00, 113.69, 90.00 |
Refinement procedure
Resolution | 19.990 - 2.400 |
R-factor | 0.232 |
Rwork | 0.232 |
R-free | 0.28200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1j42 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.700 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.400 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 56724 | |
Completeness [%] | 98.6 | 97.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | EVAPORATION |