3BWE

Crystal structure of aggregated form of DJ1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE BL-5A
Synchrotron site	Photon Factory
Beamline	BL-5A
Temperature [K]	100
Detector technology	CCD
Collection date	2004-11-04
Detector	ADSC QUANTUM 315
Wavelength(s)	1.12714
Spacegroup name	C 1 2 1
Unit cell lengths	193.616, 102.582, 85.535
Unit cell angles	90.00, 113.69, 90.00

Refinement procedure

Resolution	19.990 - 2.400
R-factor	0.232
Rwork	0.232
R-free	0.28200
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1j42
RMSD bond length	0.012
RMSD bond angle	1.700
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	AMoRE
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.400
High resolution limit [Å]	2.400	2.400
Number of reflections	56724
Completeness [%]	98.6	97.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION			EVAPORATION