3BA9

Structural Basis for Inhbition of NAD-Dependent Ligase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	BRUKER AXS MICROSTAR
Spacegroup name	C 1 2 1
Unit cell lengths	90.248, 86.277, 57.143
Unit cell angles	90.00, 101.11, 90.00

Refinement procedure

Resolution	24.330 - 1.900
Rwork	0.184
R-free	0.21600
RMSD bond length	0.006
RMSD bond angle	1.300
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	24.330
High resolution limit [Å]	1.900
Number of reflections	31586

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP			VAPOR DIFFUSION, HANGING DROP