3B6M
WrbA from Escherichia coli, second crystal form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-01-18 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54180 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 62.800, 62.800, 201.532 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.880 - 1.850 |
R-factor | 0.1885 |
Rwork | 0.187 |
R-free | 0.22344 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3b6i |
RMSD bond length | 0.019 |
RMSD bond angle | 1.671 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.940 |
High resolution limit [Å] | 1.840 | 1.840 |
Number of reflections | 35588 | |
<I/σ(I)> | 10.3 | 2.6 |
Completeness [%] | 99.4 | 97 |
Redundancy | 6.7 | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.8 | 293 | 15-30 % Polyethylene Glycol, pH 7.8, VAPOR DIFFUSION, SITTING DROP, temperature 100K, temperature 293K |