3AT3
Crystal structure of CK2alpha with pyradine derivative
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site | Photon Factory |
Beamline | BL-6A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-11-11 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 51.169, 78.483, 80.374 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.200 - 2.600 |
Rwork | 0.236 |
R-free | 0.26300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zjw |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | CNX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 56.200 |
High resolution limit [Å] | 2.600 |
Number of reflections | 10437 |
Completeness [%] | 100.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 277 | 25% ethyleneglycol, pH 8, VAPOR DIFFUSION, SITTING DROP, temperature 277K |