3AJD
Crystal structure of ATRM4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 90 |
Detector technology | CCD |
Collection date | 2007-07-10 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.00 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 40.128, 40.108, 90.559 |
Unit cell angles | 90.00, 102.75, 90.00 |
Refinement procedure
Resolution | 33.180 - 1.270 |
R-factor | 0.168 |
Rwork | 0.168 |
R-free | 0.18500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ixk |
RMSD bond length | 0.015 |
RMSD bond angle | 1.700 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.320 |
High resolution limit [Å] | 1.270 | 1.270 |
Rmerge | 0.041 | 0.335 |
Number of reflections | 72008 | |
<I/σ(I)> | 30 | 0.313 |
Completeness [%] | 98.0 | 90.8 |
Redundancy | 3.3 | 3.83 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293 | 100MM TRIS-HCL (PH 7.4), 6 % V/V 2-PROPANOL, 200MM MGCL2, 25% PEG 3350, VAPOR DIFFUSION, HANGING DROP, temperature 293K |