3A2E
Crystal structure of ginkbilobin-2, the novel antifungal protein from Ginkgo biloba seeds
Replaces: 2E79Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2006-10-28 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.00000 |
Spacegroup name | P 21 3 |
Unit cell lengths | 143.169, 143.169, 143.169 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.170 - 2.380 |
R-factor | 0.208 |
Rwork | 0.207 |
R-free | 0.23200 |
Structure solution method | MAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.001 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELXS |
Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.470 |
High resolution limit [Å] | 2.380 | 2.380 |
Total number of observations | 602150 | |
Number of reflections | 39529 | |
<I/σ(I)> | 61.2 | 8.2 |
Completeness [%] | 99.7 | |
Redundancy | 15.2 | 14.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.6 | 293 | 21% polyacrylic acid 5100, 100 mM MES, 20 mM MgCl2, pH 6.6, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
1 | VAPOR DIFFUSION, SITTING DROP | 6.6 | 293 | 21% polyacrylic acid 5100, 100 mM MES, 20 mM MgCl2, pH 6.6, VAPOR DIFFUSION, SITTING DROP, temperature 293K |