3ZHZ
Structure of Mycobacterium tuberculosis DXR in complex with a fosmidomycin analogue
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | MAX II BEAMLINE I911-2 |
| Synchrotron site | MAX II |
| Beamline | I911-2 |
| Temperature [K] | 110 |
| Detector technology | CCD |
| Collection date | 2011-06-01 |
| Detector | MARRESEARCH MX-165 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 70.040, 67.800, 85.430 |
| Unit cell angles | 90.00, 108.02, 90.00 |
Refinement procedure
| Resolution | 81.240 - 2.250 |
| R-factor | 0.20267 |
| Rwork | 0.200 |
| R-free | 0.24821 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.292 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 31.290 | 2.360 |
| High resolution limit [Å] | 2.250 | 2.250 |
| Rmerge | 0.070 | 0.310 |
| Number of reflections | 36278 | |
| <I/σ(I)> | 12.8 | 3.9 |
| Completeness [%] | 97.8 | 85 |
| Redundancy | 3.7 | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
