3WGW
Structure of PCNA bound to a small molecule inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
| Synchrotron site | Photon Factory |
| Beamline | AR-NE3A |
| Detector technology | CCD |
| Collection date | 2012-03-03 |
| Detector | ADSC QUANTUM 270 |
| Wavelength(s) | 1 |
| Spacegroup name | P 41 3 2 |
| Unit cell lengths | 192.173, 192.173, 192.173 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.800 |
| R-factor | 0.18381 |
| Rwork | 0.182 |
| R-free | 0.22125 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3vkx |
| RMSD bond length | 0.020 |
| RMSD bond angle | 2.419 |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.800 |
| Number of reflections | 30376 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
