3T12
MglA in complex with MglB in transition state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-12-18 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97700 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 106.500, 174.200, 69.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.430 - 2.200 |
R-factor | 0.19791 |
Rwork | 0.195 |
R-free | 0.24935 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1j3w |
RMSD bond length | 0.026 |
RMSD bond angle | 2.048 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.430 | 2.300 |
High resolution limit [Å] | 2.200 | 2.200 |
Number of reflections | 32905 | |
Completeness [%] | 99.4 | 98.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293.15 | 0.2M MgCl2, 0.1M Tris, 15% PEG 8000 , pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 293.15K |