3SP8
Crystal structure of NK2 in complex with fractionated Heparin DP10
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 172 |
Detector technology | PIXEL |
Collection date | 2011-01-29 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.97 |
Spacegroup name | P 61 |
Unit cell lengths | 75.980, 75.980, 199.620 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 65.800 - 1.860 |
R-factor | 0.1883 |
Rwork | 0.187 |
R-free | 0.21680 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3nh4 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.883 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 65.800 | |
High resolution limit [Å] | 1.860 | 1.860 |
Number of reflections | 54379 | |
Completeness [%] | 99.8 | 99.76 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 294 | 50mM MES pH=6.0, 30% MPD, VAPOR DIFFUSION, HANGING DROP, temperature 21K, temperature 294K |