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3S1V

Transaldolase from Thermoplasma acidophilum in complex with D-fructose 6-phosphate Schiff-base intermediate

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsBESSY BEAMLINE 14.2
Synchrotron siteBESSY
Beamline14.2
Temperature [K]100
Detector technologyCCD
Collection date2009-08-13
DetectorMARRESEARCH
Wavelength(s)0.91841
Spacegroup nameC 2 2 21
Unit cell lengths148.617, 172.535, 100.277
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution19.745 - 1.800
R-factor0.1768
Rwork0.175
R-free0.21150
Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)3s0c
RMSD bond length0.012
RMSD bond angle1.275
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHENIX
Refinement softwarePHENIX (1.6.4_486)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]19.7501.900
High resolution limit [Å]1.80030.0001.800
Rmerge0.0670.543
Number of reflections11873617640
<I/σ(I)>20.344.39
Completeness [%]99.899.9
Redundancy8.23
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1hanging drop4.5291PEG 6000, GOL, pH 4.5, hanging drop, temperature 291K

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