3R1F
Crystal structure of a key regulator of virulence in Mycobacterium tuberculosis
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.3.1 |
| Synchrotron site | ALS |
| Beamline | 8.3.1 |
| Detector technology | CCD |
| Collection date | 2010-11-17 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.11589 |
| Spacegroup name | P 32 |
| Unit cell lengths | 148.490, 148.490, 129.671 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 48.836 - 2.500 |
| R-factor | 0.1984 |
| Rwork | 0.197 |
| R-free | 0.23160 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.249 |
| Refinement software | PHENIX (1.7.1_743) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 48.850 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 104042 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 298 | 35% 5/4 PO/OH, 50 mM Hepes, 300 mM NaCl, VAPOR DIFFUSION, temperature 298K |
