Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-02-20 |
Detector | RAYONIX MX-225 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 169.290, 169.290, 184.990 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 3.970 |
High resolution limit [Å] | 3.800 | 3.800 |
Rmerge | 0.079 | 0.359 |
Number of reflections | 27116 | |
<I/σ(I)> | 12.2 | 3.2 |
Completeness [%] | 88.5 | 22.3 |
Redundancy | 5 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 1.8M Lithium sulfate, 0.05M sodium cacodylate, pH 6.0, VAPOR DIFFUSION, HANGING DROP |