3LW0

IGF-1RK in complex with ligand MSC1609119A-1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	CCD
Collection date	2007-02-08
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	1.00000
Spacegroup name	H 3
Unit cell lengths	189.346, 189.346, 115.920
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	20.000 - 1.790
Rwork	0.157
R-free	0.18500
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1jqh
RMSD bond length	0.011
RMSD bond angle	1.230
Data reduction software	XDS
Data scaling software	XSCALE
Refinement software	REFMAC (5.0)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	1.870
High resolution limit [Å]	1.790	1.790
Rmerge	0.116	0.526
Number of reflections	9614
<I/σ(I)>	11.72	4.2
Completeness [%]	99.8	99.5
Redundancy	4.8	4.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1				pH 0.0