Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-03-13 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 1.0054 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 78.894, 78.894, 93.384 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.720 - 1.800 |
| R-factor | 0.20364 |
| Rwork | 0.202 |
| R-free | 0.23963 |
| Structure solution method | UV-RIP |
| RMSD bond length | 0.028 |
| RMSD bond angle | 2.157 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SHELXD |
| Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.860 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Number of reflections | 26679 | |
| <I/σ(I)> | 31.5 | 3 |
| Completeness [%] | 97.7 | 82.3 |
| Redundancy | 9.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 293 | 1.9 M SODIUM/POTASSIUM PHOSPHATE, pH 6.4, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 293 | 1.9 M SODIUM/POTASSIUM PHOSPHATE, pH 6.4, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
