3KLM
17beta-HSD1 in complex with DHT
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X12B |
| Synchrotron site | NSLS |
| Beamline | X12B |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 4 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 123.246, 43.360, 60.398 |
| Unit cell angles | 90.00, 100.18, 90.00 |
Refinement procedure
| Resolution | 30.330 - 1.700 |
| R-factor | 0.21899 |
| Rwork | 0.217 |
| R-free | 0.25666 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.779 |
| Data reduction software | d*TREK |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.330 |
| High resolution limit [Å] | 1.700 |
| Number of reflections | 34119 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | VAPOR DIFFUSION, HANGING DROP |
