3K35
Crystal Structure of Human SIRT6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2009-07-30 |
Detector | RIGAKU RAXIS |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 89.388, 136.266, 89.260 |
Unit cell angles | 90.00, 119.87, 90.00 |
Refinement procedure
Resolution | 19.950 - 2.000 |
R-factor | 0.2022 |
Rwork | 0.202 |
R-free | 0.26723 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1yc5 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.506 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 100.000 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.086 |
Number of reflections | 120514 |
<I/σ(I)> | 9.5 |
Completeness [%] | 97.1 |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.8 | 293 | 2M NH4SO4, 2%PEG400, 0.1M Bis-Tris pH 5.8, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K |