3IJ2
Ligand-receptor structure
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.2.2 |
| Synchrotron site | ALS |
| Beamline | 8.2.2 |
| Collection date | 2007-01-01 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 145.406, 145.406, 114.252 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 47.595 - 3.750 |
| R-factor | 0.2565 |
| Rwork | 0.256 |
| R-free | 0.27390 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.568 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | PHENIX (1.4_153) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 3.750 |
| Number of reflections | 14644 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
