3I7I

MMP-13 in complex with a non zinc-chelating inhibitor

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Detector technology	CCD
Detector	MARMOSAIC 225 mm CCD
Spacegroup name	C 1 2 1
Unit cell lengths	134.186, 35.777, 95.295
Unit cell angles	90.00, 131.08, 90.00

Refinement procedure

Resolution	30.862 - 2.208
R-factor	0.235
Rwork	0.230
R-free	0.31400
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.993
Refinement software	PHENIX (1.4_6)

Data quality characteristics

	Overall
Low resolution limit [Å]	66.960
High resolution limit [Å]	2.208
Number of reflections	17300

Crystallization Conditions

crystal ID	method	pH	temperature	details
1