3HWN
CATHEPSIN L with AZ13010160
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2007-11-15 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 1.0005 |
| Spacegroup name | P 1 |
| Unit cell lengths | 57.070, 62.800, 67.970 |
| Unit cell angles | 105.34, 94.04, 115.26 |
Refinement procedure
| Resolution | 35.810 - 2.330 |
| R-factor | 0.25206 |
| Rwork | 0.250 |
| R-free | 0.34718 |
| Structure solution method | OTHER |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.340 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 35.810 | 2.390 |
| High resolution limit [Å] | 2.330 | 2.330 |
| Rmerge | 0.098 | 0.209 |
| Number of reflections | 31593 | |
| Completeness [%] | 91.7 | 81.9 |
| Redundancy | 2 | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 298 | PEG, pH 7.4, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
