3FZJ
TsaR low resolution crystal structure, tetragonal form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-2 |
| Synchrotron site | ESRF |
| Beamline | ID14-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-06-27 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.9326 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 204.370, 204.370, 336.210 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 42.340 - 7.100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3fxq |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.570 | 7.100 |
| High resolution limit [Å] | 7.000 | 7.000 |
| Rmerge | 0.109 | 0.662 |
| Number of reflections | 11779 | |
| <I/σ(I)> | 17.09 | 2.74 |
| Completeness [%] | 99.3 | 100 |
| Redundancy | 7.73 | 8.15 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8.5 | 298 | 2M Ammonium phosphate, 0.1M Tris-HCl, pH 8.5, microbatch under oil, temperature 298K |
