3E3N
The Glycogen phosphorylase b R state- AMP complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2002-11-24 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.87 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 119.019, 188.079, 175.913 |
Unit cell angles | 90.00, 108.92, 90.00 |
Refinement procedure
Resolution | 29.790 - 2.700 |
R-factor | 0.19517 |
Rwork | 0.192 |
R-free | 0.25609 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1abb |
RMSD bond length | 0.009 |
RMSD bond angle | 1.297 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.850 | 2.750 |
High resolution limit [Å] | 2.700 | 2.700 |
Number of reflections | 189160 | |
<I/σ(I)> | 6.2 | 1.67 |
Completeness [%] | 94.3 | 92.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICRODIALYSIS | 7.5 | 289 | 1.2-1.4 M ammonium sulphate, pH 7.5, MICRODIALYSIS, temperature 289K |