3DXC
Crystal structure of the intracellular domain of human APP in complex with Fe65-PTB2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-07-19 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.00 |
Spacegroup name | P 61 |
Unit cell lengths | 114.320, 114.320, 74.850 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 33.000 - 2.100 |
R-factor | 0.20449 |
Rwork | 0.202 |
R-free | 0.23816 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.312 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.3.0008) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.000 | 2.210 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.060 | 0.465 |
Number of reflections | 32612 | |
<I/σ(I)> | 28.8 | 4.7 |
Completeness [%] | 100.0 | |
Redundancy | 11.1 | 11.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.6 | 293 | 3.2 M NaCl,0.1 M sodium acetate , pH 4.6, VAPOR DIFFUSION, temperature 293K |