3D5K
Crystal structure of the OprM channel in a non-symmetrical space group
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-08-26 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.931 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 73.900, 70.200, 344.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.000 - 2.400 |
R-factor | 0.23996 |
Rwork | 0.236 |
R-free | 0.29320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1wp1 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.888 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.710 | 2.540 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 69761 | |
Completeness [%] | 98.7 | 94.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 291 | Sodium citrate 1M, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |