Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

3B6M

WrbA from Escherichia coli, second crystal form

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2007-01-18
DetectorMAR scanner 345 mm plate
Wavelength(s)1.54180
Spacegroup nameP 43 21 2
Unit cell lengths62.800, 62.800, 201.532
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution45.880 - 1.850
R-factor0.1885
Rwork0.187
R-free0.22344
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3b6i
RMSD bond length0.019
RMSD bond angle1.671
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareMOLREP
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.940
High resolution limit [Å]1.8401.840
Number of reflections35588
<I/σ(I)>10.32.6
Completeness [%]99.497
Redundancy6.76.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.829315-30 % Polyethylene Glycol, pH 7.8, VAPOR DIFFUSION, SITTING DROP, temperature 100K, temperature 293K

219869

PDB entries from 2024-05-15

PDB statisticsPDBj update infoContact PDBjnumon