3AYU
Crystal structure of MMP-2 active site mutant in complex with APP-drived decapeptide inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | Cu FINE FOCUS |
| Wavelength(s) | 1.54180 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 61.881, 76.060, 37.082 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.000 |
| R-factor | 0.16229 |
| Rwork | 0.160 |
| R-free | 0.20455 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.091 |
| Refinement software | REFMAC (5.6.0085) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 12160 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
