Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

366D

1.3 A STRUCTURE DETERMINATION OF THE D(CG(5-BRU)ACG)2/6-BROMO-9-AMINO-DACA COMPLEX

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsELETTRA BEAMLINE 5.2R
Synchrotron siteELETTRA
Beamline5.2R
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date1997-10-14
DetectorMARRESEARCH
Spacegroup nameP 64
Unit cell lengths30.110, 30.110, 39.560
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution8.000 - 1.300
Structure solution methodAB INITIO
RMSD bond length0.002
RMSD bond angle0.020
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareSHELXS
Refinement softwareSHELXL-96
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]8.000
High resolution limit [Å]1.3001.300

*

Rmerge0.068

*

Total number of observations31514

*

Number of reflections9306

*

Completeness [%]95.337

*

Redundancy3.91
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, sitting drop

*

6.5285

*

pH 6.5, VAPOR DIFFUSION, HANGING DROP
Crystallization Reagents
IDcrystal IDsolution IDreagent nameconcentrationdetails
111SODIUM CACODYLATE
211MGCL2
311SPERMINE
411MPD
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropDNA0.5 (mM)
21dropcacodylate50 (mM)
31dropmagnesium acetate2.0 (mM)
41dropsperine-4HCl3.0 (mM)
51dropMPD5 (%)
61reservoirMPD30 (%)

217705

PDB entries from 2024-03-27

PDB statisticsPDBj update infoContact PDBjnumon