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2ZW0

Crystal structure of a Streptococcal protein G B1 mutant

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-17A
Synchrotron sitePhoton Factory
BeamlineBL-17A
Detector technologyCCD
Collection date2007-05-24
DetectorADSC QUANTUM 270
Wavelength(s)1.000
Spacegroup nameC 2 2 21
Unit cell lengths25.764, 36.360, 93.688
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution20.000 - 1.400
R-factor0.17865
Rwork0.176
R-free0.22350
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.009
RMSD bond angle1.216
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]1.400
Number of reflections9052
Redundancy6.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1

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