2ZOL
Crystal structure of H-2Db in complex with the W513S variant of JHMV epitope S510
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-07-20 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.999 |
Spacegroup name | P 1 2 1 |
Unit cell lengths | 83.561, 71.033, 86.999 |
Unit cell angles | 90.00, 103.45, 90.00 |
Refinement procedure
Resolution | 33.700 - 2.700 |
R-factor | 0.2564 |
Rwork | 0.254 |
R-free | 0.30726 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bz9 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.960 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.390 | 2.850 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.083 | 0.330 |
Number of reflections | 27219 | |
<I/σ(I)> | 8.2 | 3.2 |
Completeness [%] | 99.3 | 99.1 |
Redundancy | 3 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 294 | 0.1M sodium citrate, 28% PEG 3350, 0.15M lithium sulfate, pH 6.4, VAPOR DIFFUSION, HANGING DROP, temperature 294K |