2YKB
Tricyclic series of Hsp90 inhibitors
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Collection date | 2004-12-09 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 66.348, 90.627, 98.638 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.990 - 1.930 |
R-factor | 0.2015 |
Rwork | 0.199 |
R-free | 0.24110 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.100 |
Data reduction software | PROCESS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | BUSTER (2.9.7) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.050 | 2.030 |
High resolution limit [Å] | 1.930 | 1.930 |
Rmerge | 0.100 | 0.390 |
Number of reflections | 21509 | |
Completeness [%] | 94.8 | 94.8 |
Redundancy | 4 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | pH 7.5 |