2YIW
triazolopyridine inhibitors of p38 kinase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 64.580, 74.320, 76.820 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 18.060 - 2.000 |
R-factor | 0.2227 |
Rwork | 0.221 |
R-free | 0.25940 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.080 |
Refinement software | BUSTER (2.9.6) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 18.000 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.050 |
Number of reflections | 253061 |
Completeness [%] | 99.4 |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |