2YGP
WIF domain-EGF-like domain 1 Met77Trp of human Wnt inhibitory factor 1 in complex with 1,2-dipalmitoylphosphatidylcholine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | C 2 2 2 |
Unit cell lengths | 50.760, 134.241, 60.193 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.316 - 2.222 |
R-factor | 0.1875 |
Rwork | 0.185 |
R-free | 0.22890 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 2.217 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.320 | 2.280 |
High resolution limit [Å] | 2.220 | 2.220 |
Rmerge | 0.090 | 0.570 |
Number of reflections | 10433 | |
<I/σ(I)> | 12.7 | 2.3 |
Completeness [%] | 99.4 | 92 |
Redundancy | 6.4 | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 1.1 M DIAMMONIUM TARTRATE, PH 7.0, 20 MM SPERMIDINE, 0.5 MM CACL2 |