2Y95

Solution structure of AUCG tetraloop hairpin found in human Xist RNA A-repeats essential for X-inactivation

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	DRX		800
2	Bruker	DRX		900
3	Bruker	DRX		600
4	Bruker	DRX		600
5	Bruker	DRX		600
6	Bruker	DRX		600
7	Bruker	DRX		900
8	Bruker	DMX		800
9	Bruker	DRX		600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-1H NOESY WITH WATERGATE AND WATERFLIPBACK
10	6	1	3D HCCH-E.COSY
11	6	1	3D HCCH-TOCSY
12	6	1	3D HCN
13	6	1	3D FORWARD DIRECTED HCCH-E.COSY
14	6	1	HNN- COSY LONG-RANGE
15	6	1	HNN-COSY WITH ADIABATIC REFOCUSING
16	6	1	TROSY RELAYED HCCH-COSY
17	7	1	2D 1H-13C HMQC
18	7	1	3D 1H-13C NOESY-HMQC
19	7	1	3D HCP
2	2	1	2D 1H-13C HSQC
20	7	1	3D HCP SPIN-ECHO-DIFF
21	8	1	3D HCCH-COSY
22	9	1	2D 1H-13C HC-TROSY
3	2	1	2D 1H-1H NOESY
4	3	1	2D 1H-13C HC-TROSY
5	3	1	2D 1H-1H TOCSY
6	4	1	2D 1H-15N HSQC
7	4	1	HNN-COSY
8	5	1	HNN-COSY
9	6	1	2D 1H-13C SELECTIVE HSQC

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6	1.0	278
2	6	1.0	298
3	6	1.0	298
4	6	1.0	278
5	6	1.0	278
6	6	1.0	298
7	6	1.0	298
8	6	1.0	298
9	6	1.0	298

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	10