2Y5G
FACTOR XA - CATION INHIBITOR COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-04-23 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.946, 74.353, 77.029 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.880 - 1.290 |
R-factor | 0.14747 |
Rwork | 0.145 |
R-free | 0.18555 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2jkh |
RMSD bond length | 0.013 |
RMSD bond angle | 1.703 |
Data reduction software | XDS |
Data scaling software | SADABS |
Phasing software | CCP4 |
Refinement software | REFMAC (5.6.0093) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.310 |
High resolution limit [Å] | 1.290 | 1.290 |
Rmerge | 0.050 | 0.790 |
Number of reflections | 71402 | |
<I/σ(I)> | 15.74 | 1.25 |
Completeness [%] | 99.9 | 99.8 |
Redundancy | 7.21 | 7.08 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |