2Y3V
N-terminal head domain of Danio rerio SAS-6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2009-12-12 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 66.990, 95.270, 129.060 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.799 - 1.920 |
R-factor | 0.227 |
Rwork | 0.226 |
R-free | 0.24650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | SE-MET DERIVATIVE |
RMSD bond length | 0.002 |
RMSD bond angle | 0.663 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.800 | 2.020 |
High resolution limit [Å] | 1.920 | 1.920 |
Rmerge | 0.130 | 1.500 |
Number of reflections | 63745 | |
<I/σ(I)> | 12.4 | 1.8 |
Completeness [%] | 99.4 | 98.6 |
Redundancy | 12.3 | 11.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 0.1 M TRIS PH 8.5, 25% PEG 3350. |