2XZP
Upf1 helicase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-06-25 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 3 |
Unit cell lengths | 146.120, 146.120, 146.120 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 84.362 - 2.720 |
R-factor | 0.1751 |
Rwork | 0.173 |
R-free | 0.21410 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2wjv |
RMSD bond length | 0.009 |
RMSD bond angle | 0.785 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 84.360 | 2.870 |
High resolution limit [Å] | 2.720 | 2.720 |
Rmerge | 0.060 | 0.640 |
Number of reflections | 28118 | |
<I/σ(I)> | 32.2 | 4.4 |
Completeness [%] | 99.8 | 98.7 |
Redundancy | 13.4 | 13.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 50MM SODIUM CITRATE PH 6.0, 1.5M SODIUM MALONATE |