2XZ0
The Structure of the 2:1 (Partially Occupied) Complex Between Stearoyl Acyl Carrier Protein Desaturase from Ricinus Communis (Castor Bean) and Acyl Carrier Protein.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Detector | MAR555 FLAT PANEL |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 188.274, 188.274, 81.315 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.280 - 3.000 |
R-factor | 0.24434 |
Rwork | 0.243 |
R-free | 0.27744 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1afr |
RMSD bond length | 0.013 |
RMSD bond angle | 1.299 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 3.160 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.080 | 0.480 |
Number of reflections | 33376 | |
<I/σ(I)> | 21.9 | 4.3 |
Completeness [%] | 99.9 | 100 |
Redundancy | 11.1 | 9.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.62 | 4-5% PEG 20000, 8% PEG 550MME, 180MM SODIUM BROMIDE, 100MM SODIUM ACETATE PH 5.62, 15% GLYCEROL. |