2XJC
Crystal structure of the D52N variant of cytosolic 5'-nucleotidase II in complex with guanosine monophosphate and diadenosine tetraphosphate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2008-01-30 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 91.540, 127.360, 130.240 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.790 - 2.000 |
R-factor | 0.17801 |
Rwork | 0.176 |
R-free | 0.21893 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2jcm |
RMSD bond length | 0.016 |
RMSD bond angle | 1.588 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.200 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.080 | 0.440 |
Number of reflections | 51649 | |
<I/σ(I)> | 17.37 | 4.1 |
Completeness [%] | 99.9 | 100 |
Redundancy | 5.6 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.1 M BICINE PH 9.0, 10% PEG6000 |