2XBM
Crystal structure of the dengue virus methyltransferase bound to a 5'- capped octameric RNA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 77 |
| Detector technology | PIXEL |
| Collection date | 2009-03-06 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 32 |
| Unit cell lengths | 137.543, 137.543, 109.385 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 39.710 - 2.900 |
| R-factor | 0.205 |
| Rwork | 0.204 |
| R-free | 0.23100 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.211 |
| Data reduction software | MOSFLM |
| Data scaling software | CCP4 |
| Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 60.000 | |
| High resolution limit [Å] | 2.900 | 2.900 |
| Rmerge | 0.100 | |
| Number of reflections | 50667 | |
| <I/σ(I)> | 2.2 | |
| Completeness [%] | 99.0 | |
| Redundancy | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5 | PH 5 |
