2XAG
Crystal structure of LSD1-CoREST in complex with para-bromo-(-)-trans- 2-phenylcyclopropyl-1-amine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 116.470, 178.030, 236.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 71.960 - 3.100 |
R-factor | 0.20988 |
Rwork | 0.209 |
R-free | 0.24470 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.541 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.5.0090) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 3.100 |
Rmerge | 0.100 |
Number of reflections | 42608 |
<I/σ(I)> | 5.6 |
Completeness [%] | 95.7 |
Redundancy | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SODIUM-POTASSIUM TARTRATE, ADA BUFFER PH 6.5 |