2X75
Staphylococcus aureus adenylosuccinate lyase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-12-16 |
Detector | ADSC CCD |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 81.647, 121.265, 105.727 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.000 - 2.500 |
R-factor | 0.21772 |
Rwork | 0.214 |
R-free | 0.28474 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1c3c |
RMSD bond length | 0.010 |
RMSD bond angle | 1.160 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 97.000 | 2.640 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.050 | 0.490 |
Number of reflections | 17795 | |
<I/σ(I)> | 14.3 | 2.6 |
Completeness [%] | 96.9 | 98.7 |
Redundancy | 5.3 | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |