2X4M
Yersinia Pestis Plasminogen Activator Pla
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 69.913, 127.824, 107.175 |
Unit cell angles | 90.00, 90.06, 90.00 |
Refinement procedure
Resolution | 19.930 - 2.550 |
R-factor | 0.186 |
Rwork | 0.185 |
R-free | 0.24600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.267 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.580 |
High resolution limit [Å] | 2.550 | 2.540 |
Rmerge | 0.100 | |
Number of reflections | 56736 | |
<I/σ(I)> | 1.93 | |
Completeness [%] | 95.7 | 79.2 |
Redundancy | 6.3 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 3.5 | 16% PEG 400, 0.1M LITHIUM CITRATE PH: 3.5 |