2X2C
acetyl-CypA:cyclosporine complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 287 |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 107.429, 107.429, 428.871 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 61.270 - 2.410 |
| R-factor | 0.20917 |
| Rwork | 0.206 |
| R-free | 0.26363 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.020 |
| RMSD bond angle | 1.759 |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 57.000 |
| High resolution limit [Å] | 2.400 |
| Rmerge | 0.150 |
| Number of reflections | 58013 |
| <I/σ(I)> | 5.7 |
| Completeness [%] | 98.2 |
| Redundancy | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
