2WZX
AMP-C BETA-LACTAMASE (PSEUDOMONAS AERUGINOSA)IN COMPLEX WITH compound M-02
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2006-07-14 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.759, 72.135, 105.933 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 59.620 - 1.400 |
R-factor | 0.18263 |
Rwork | 0.182 |
R-free | 0.19799 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.230 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | HKL-2000 |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.420 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.060 | 0.450 |
Number of reflections | 65910 | |
<I/σ(I)> | 27.6 | 2.1 |
Completeness [%] | 96.3 | 69.2 |
Redundancy | 6.9 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |