2WQ9
Crystal Structure of RBP4 bound to Oleic Acid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 105 |
Spacegroup name | H 3 |
Unit cell lengths | 103.060, 103.060, 72.710 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 56.340 - 1.650 |
R-factor | 0.18924 |
Rwork | 0.188 |
R-free | 0.21919 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qab |
RMSD bond length | 0.009 |
RMSD bond angle | 1.116 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.750 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.040 | 0.420 |
Number of reflections | 34250 | |
<I/σ(I)> | 16.96 | 2.82 |
Completeness [%] | 98.8 | 99.8 |
Redundancy | 3.4 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 3.5 TO 4.2 M NACL, 1M HEPES PH 7.2 |