2WOJ
ADP-AlF4 complex of S. cerevisiae GET3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-G |
Synchrotron site | APS |
Beamline | 21-ID-G |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-08-10 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.612, 82.628, 167.282 |
Unit cell angles | 90.00, 98.28, 90.00 |
Refinement procedure
Resolution | 37.441 - 1.994 |
R-factor | 0.1778 |
Rwork | 0.176 |
R-free | 0.21270 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PARTIAL MODEL DERIVED FROM SAD DATASET |
RMSD bond length | 0.011 |
RMSD bond angle | 1.331 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.060 | 0.590 |
Number of reflections | 94446 | |
<I/σ(I)> | 21.1 | 1.9 |
Completeness [%] | 95.9 | 86.3 |
Redundancy | 3.6 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.4 | 33% PEG3350, 0.1 M TRIS PH 8.4, 0.2 M AMMONIUM ACETATE, 75 MM NA/K TARTRATE |