2WNP
M-ficolin mutant Y271F
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Temperature [K] | 77.36 |
Collection date | 2008-11-29 |
Detector | MARRESEARCH |
Spacegroup name | H 3 |
Unit cell lengths | 73.550, 73.550, 124.760 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 27.540 - 1.210 |
R-factor | 0.17839 |
Rwork | 0.178 |
R-free | 0.19137 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2jhm |
RMSD bond length | 0.007 |
RMSD bond angle | 1.108 |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.240 |
High resolution limit [Å] | 1.210 | 1.210 |
Rmerge | 0.050 | 0.580 |
Number of reflections | 54807 | |
<I/σ(I)> | 28.27 | 2.37 |
Completeness [%] | 72.0 | 7.3 |
Redundancy | 9.7 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |