2WNH
Crystal Structure Analysis of Klebsiella sp ASR1 Phytase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-01-14 |
Detector | MARRESEARCH |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 133.680, 133.680, 111.240 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 94.490 - 1.680 |
R-factor | 0.18249 |
Rwork | 0.181 |
R-free | 0.20744 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.012 |
RMSD bond angle | 1.315 |
Data reduction software | XDS |
Data scaling software | SCALEPACK |
Phasing software | SOLVE (RESOLVE) |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 94.490 | 1.750 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.070 | 0.410 |
Number of reflections | 113622 | |
<I/σ(I)> | 15 | 2.6 |
Completeness [%] | 94.1 | 72.9 |
Redundancy | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4 M SODIUM FORMATE |