2WGF
Crystal structure of Mycobacterium tuberculosis C171Q KasA variant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector | RIGAKU |
Spacegroup name | P 31 |
Unit cell lengths | 151.505, 151.505, 147.839 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 33.710 - 2.150 |
R-factor | 0.168 |
Rwork | 0.166 |
R-free | 0.21100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2wgd |
RMSD bond length | 0.005 |
RMSD bond angle | 0.917 |
Data reduction software | MOSFLM |
Data scaling software | TRUNCATE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.710 | 2.170 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.080 | 0.480 |
Number of reflections | 335101 | |
<I/σ(I)> | 9.64 | 1.6 |
Completeness [%] | 97.9 | 96.2 |
Redundancy | 1.7 | 1.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | PEG3350, POTASSIUM FORMATE |